Novel Optical Techniques with Application in Temperature Unduced Thermal Displacement and Pressure Induced Phase Transformation in DAC Cell

Zhongwu Wang, Xincheng Yao, Yusheng Zhao and David Schiferl

Los Alamos National Laboratory

z_wang@lanl.gov

We designed an optical lever to measure the temperature induced thermal displacement of solids, especially for nanocrystals. The sample and a knife-edge as a reference point are connected by a strip of aluminized mylar, which is served as a mirror. A Position Sensitive Photodiode (PSD) was used to record the deflection of the laser beam, which was induced by heating or cooling sample. Such a technique allows us to measure the temperature-induced displacement with the resolution of 1 nm. Furthermore, the Laser Polarized Sensitive Optical Coherence Topography (LPSOCT) was developed to measure the pressure induced phase transformation in Diamond Anvil Cell (DAC). A low coherence laser (SLD) was split to the two beams by an optical prism: one was focused on the sample, and another one was used as a reference. The interference signal between the reflected and reference beam was recorded by a fast photodiode, demodulated by a lock-in amplifier and continuously digitized by AID to computer. As the phase transition occurs, the variation of anistropic properties results in a significant change of the polarisity of the interference signal. Now we are testing several samples, and the preliminary results will be presented.